Table 4. Experimental details.

Crystal data
Chemical formula	C22H33N3O4
M r	403.51
Crystal system, space group	Triclinic, P
Temperature (K)	100
a, b, c (Å)	9.6579 (19), 11.798 (2), 12.216 (2)
α, β, γ (°)	100.95 (3), 109.41 (3), 111.12 (3)
V (Å3)	1146.3 (7)
Z	2
Radiation type	Synchrotron, λ = 0.96990 Å
μ (mm−1)	0.17
Crystal size (mm)	0.25 × 0.15 × 0.12
Data collection
Diffractometer	Rayonix SX165 CCD
Absorption correction	Multi-scan (SCALA; Evans, 2006 ▸)
T min, T max	0.950, 0.970
No. of measured, independent and observed [I > 2σ(I)] reflections	14236, 4609, 3323
R int	0.081
(sin θ/λ)max (Å−1)	0.642
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.067, 0.180, 1.04
No. of reflections	4609
No. of parameters	270
H-atom treatment	H-atom parameters constrained
Δρmax, Δρmin (e Å−3)	0.36, −0.32

Computer programs: Marccd (Doyle, 2011 ▸), iMosflm (Battye et al., 2011 ▸), SHELXT (Sheldrick, 2015a ▸), SHELXL (Sheldrick, 2015b ▸), ORTEP-3 for Windows (Farrugia, 2012 ▸) and PLATON (Spek, 2020 ▸).