Table 2.
ΔP (bar) | Passes | WPI concentration (%) | X1 | X2 | X3 | X1X1 | X2X2 | X3X3 | X1X2 | X2X3 | X3X1 | Soluble proteins content (mg/mL) | Degree of hydrolysis (%) |
---|---|---|---|---|---|---|---|---|---|---|---|---|---|
5 | 0 | 1.5 | −1 | −1 | −1 | 1 | 1 | 1 | 1 | 1 | 1 | 3.76 ± 0.41 | 27.26 ± 1.28 |
5 | 5 | 1.5 | −1 | −0.67 | −1 | 1 | 0.44 | 1 | 0.67 | 0.67 | 1 | 4.21 ± 0.37 | 30.51 ± 1.35 |
5 | 10 | 1.5 | −1 | −0.33 | −1 | 1 | 0.11 | 1 | 0.33 | 0.33 | 1 | 4.98 ± 0.36 | 36.09 ± 1.08 |
5 | 15 | 1.5 | −1 | 0 | −1 | 1 | 0 | 1 | 0 | 0 | 1 | 6.02 ± 0.37 | 43.62 ± 1.98 |
5 | 20 | 1.5 | −1 | 0.33 | −1 | 1 | 0.11 | 1 | −0.33 | −0.33 | 1 | 6.89 ± 0.40 | 49.93 ± 1.86 |
5 | 25 | 1.5 | −1 | 0.67 | −1 | 1 | 0.44 | 1 | −0.67 | −0.67 | 1 | 7.54 ± 0.45 | 54.64 ± 1.59 |
5 | 30 | 1.5 | −1 | 1 | −1 | 1 | 1 | 1 | −1 | −1 | 1 | 8.32 ± 0.55 | 60.29 ± 2.15 |
6 | 0 | 1.5 | −0.33 | −1 | −1 | 0.11 | 1 | 1 | 0.33 | 1 | 0.33 | 3.76 ± 0.41 | 27.26 ± 1.28 |
6 | 5 | 1.5 | −0.33 | −0.67 | −1 | 0.11 | 0.44 | 1 | 0.22 | 0.67 | 0.33 | 4.8 ± 0.44 | 34.78 ± 1.86 |
6 | 10 | 1.5 | −0.33 | −0.33 | −1 | 0.11 | 0.11 | 1 | 0.11 | 0.33 | 0.33 | 5.35 ± 0.42 | 38.77 ± 1.98 |
6 | 15 | 1.5 | −0.33 | 0 | −1 | 0.11 | 0 | 1 | 0 | 0 | 0.33 | 6.58 ± 0.43 | 47.68 ± 2.18 |
6 | 20 | 1.5 | −0.33 | 0.33 | −1 | 0.11 | 0.11 | 1 | −0.11 | −0.33 | 0.33 | 7.44 ± 0.40 | 53.91 ± 2.64 |
6 | 25 | 1.5 | −0.33 | 0.67 | −1 | 0.11 | 0.44 | 1 | −0.22 | −0.67 | 0.33 | 8.05 ± 0.47 | 58.33 ± 3.06 |
6 | 30 | 1.5 | −0.33 | 1 | −1 | 0.11 | 1 | 1 | −0.33 | −1 | 0.33 | 9.25 ± 0.55 | 67.02 ± 2.66 |
7 | 0 | 1.5 | 0.33 | −1 | −1 | 0.11 | 1 | 1 | −0.33 | 1 | −0.33 | 3.76 ± 0.41 | 27.26 ± 1.28 |
7 | 5 | 1.5 | 0.33 | −0.67 | −1 | 0.11 | 0.44 | 1 | −0.22 | 0.67 | −0.33 | 5.39 ± 0.46 | 39.06 ± 1.98 |
7 | 10 | 1.5 | 0.33 | −0.33 | −1 | 0.11 | 0.11 | 1 | −0.11 | 0.33 | −0.33 | 6.27 ± 0.43 | 45.43 ± 1.31 |
7 | 15 | 1.5 | 0.33 | 0 | −1 | 0.11 | 0 | 1 | 0 | 0 | −0.33 | 7.45 ± 0.41 | 53.99 ± 1.24 |
7 | 20 | 1.5 | 0.33 | 0.33 | −1 | 0.11 | 0.11 | 1 | 0.11 | −0.33 | −0.33 | 9.1 ± 0.43 | 65.94 ± 2.21 |
7 | 25 | 1.5 | 0.33 | 0.67 | −1 | 0.11 | 0.44 | 1 | 0.22 | −0.67 | −0.33 | 10.35 ± 0.47 | 75.00 ± 2.45 |
7 | 30 | 1.5 | 0.33 | 1 | −1 | 0.11 | 1 | 1 | 0.33 | −1 | −0.33 | 11.15 ± 0.55 | 80.80 ± 2.61 |
8 | 0 | 1.5 | 1 | −1 | −1 | 1 | 1 | 1 | −1 | 1 | −1 | 3.76 ± 0.41 | 27.26 ± 1.28 |
8 | 5 | 1.5 | 1 | −0.67 | −1 | 1 | 0.44 | 1 | −0.67 | 0.67 | −1 | 6.12 ± 0.53 | 44.35 ± 1.63 |
8 | 10 | 1.5 | 1 | −0.33 | −1 | 1 | 0.11 | 1 | −0.33 | 0.33 | −1 | 7.46 ± 0.49 | 54.06 ± 1.69 |
8 | 15 | 1.5 | 1 | 0 | −1 | 1 | 0 | 1 | 0 | 0 | −1 | 8.63 ± 0.48 | 62.54 ± 1.28 |
8 | 20 | 1.5 | 1 | 0.33 | −1 | 1 | 0.11 | 1 | 0.33 | −0.33 | −1 | 12.02 ± 0.49 | 87.10 ± 2.34 |
8 | 25 | 1.5 | 1 | 0.67 | −1 | 1 | 0.44 | 1 | 0.67 | −0.67 | −1 | 12.23 ± 0.53 | 88.62 ± 2.50 |
8 | 30 | 1.5 | 1 | 1 | −1 | 1 | 1 | 1 | 1 | −1 | −1 | 12.31 ± 0.62 | 89.20 ± 2.46 |
5 | 0 | 3 | −1 | −1 | 0 | 1 | 1 | 0 | 1 | 0 | 0 | 7.82 ± 0.37 | 28.33 ± 1.17 |
5 | 5 | 3 | −1 | −0.67 | 0 | 1 | 0.44 | 0 | 0.67 | 0 | 0 | 9.58 ± 0.31 | 34.71 ± 1.22 |
5 | 10 | 3 | −1 | −0.33 | 0 | 1 | 0.11 | 0 | 0.33 | 0 | 0 | 10.95 ± 0.30 | 39.67 ± 1.40 |
5 | 15 | 3 | −1 | 0 | 0 | 1 | 0 | 0 | 0 | 0 | 0 | 12.76 ± 0.32 | 46.23 ± 1.65 |
5 | 20 | 3 | −1 | 0.33 | 0 | 1 | 0.11 | 0 | −0.33 | 0 | 0 | 13.83 ± 0.33 | 50.11 ± 1.78 |
5 | 25 | 3 | −1 | 0.67 | 0 | 1 | 0.44 | 0 | −0.67 | 0 | 0 | 14.11 ± 0.38 | 51.12 ± 1.56 |
5 | 30 | 3 | −1 | 1 | 0 | 1 | 1 | 0 | −1 | 0 | 0 | 14.29 ± 0.48 | 51.77 ± 1.44 |
6 | 0 | 3 | −0.33 | −1 | 0 | 0.11 | 1 | 0 | 0.33 | 0 | 0 | 7.82 ± 0.37 | 28.33 ± 1.17 |
6 | 5 | 3 | −0.33 | −0.67 | 0 | 0.11 | 0.44 | 0 | 0.22 | 0 | 0 | 14.48 ± 0.36 | 52.46 ± 1.36 |
6 | 10 | 3 | −0.33 | −0.33 | 0 | 0.11 | 0.11 | 0 | 0.11 | 0 | 0 | 15.05 ± 0.31 | 54.53 ± 1.51 |
6 | 15 | 3 | −0.33 | 0 | 0 | 0.11 | 0 | 0 | 0 | 0 | 0 | 15.85 ± 0.30 | 57.43 ± 1.80 |
6 | 20 | 3 | −0.33 | 0.33 | 0 | 0.11 | 0.11 | 0 | −0.11 | 0 | 0 | 16.61 ± 0.32 | 60.18 ± 1.72 |
6 | 25 | 3 | −0.33 | 0.67 | 0 | 0.11 | 0.44 | 0 | −0.22 | 0 | 0 | 16.85 ± 0.38 | 61.05 ± 2.01 |
6 | 30 | 3 | −0.33 | 1 | 0 | 0.11 | 1 | 0 | −0.33 | 0 | 0 | 17.02 ± 0.50 | 61.67 ± 1.58 |
7 | 0 | 3 | 0.33 | −1 | 0 | 0.11 | 1 | 0 | −0.33 | 0 | 0 | 7.82 ± 0.37 | 28.33 ± 1.17 |
7 | 5 | 3 | 0.33 | −0.67 | 0 | 0.11 | 0.44 | 0 | −0.22 | 0 | 0 | 15.3 ± 0.38 | 55.43 ± 1.48 |
7 | 10 | 3 | 0.33 | −0.33 | 0 | 0.11 | 0.11 | 0 | −0.11 | 0 | 0 | 16.42 ± 0.32 | 59.49 ± 2.12 |
7 | 15 | 3 | 0.33 | 0 | 0 | 0.11 | 0 | 0 | 0 | 0 | 0 | 17.51 ± 0.30 | 63.44 ± 2.60 |
7 | 20 | 3 | 0.33 | 0.33 | 0 | 0.11 | 0.11 | 0 | 0.11 | 0 | 0 | 17.85 ± 0.31 | 64.67 ± 2.11 |
7 | 25 | 3 | 0.33 | 0.67 | 0 | 0.11 | 0.44 | 0 | 0.22 | 0 | 0 | 18.03 ± 0.36 | 65.33 ± 2.66 |
7 | 30 | 3 | 0.33 | 1 | 0 | 0.11 | 1 | 0 | 0.33 | 0 | 0 | 18.27 ± 0.47 | 66.19 ± 2.74 |
8 | 0 | 3 | 1 | −1 | 0 | 1 | 1 | 0 | −1 | 0 | 0 | 7.82 ± 0.37 | 28.33 ± 1.17 |
8 | 5 | 3 | 1 | −0.67 | 0 | 1 | 0.44 | 0 | −0.67 | 0 | 0 | 16.26 ± 0.55 | 58.91 ± 2.86 |
8 | 10 | 3 | 1 | −0.33 | 0 | 1 | 0.11 | 0 | −0.33 | 0 | 0 | 17.32 ± 0.50 | 62.75 ± 2.59 |
8 | 15 | 3 | 1 | 0 | 0 | 1 | 0 | 0 | 0 | 0 | 0 | 18.05 ± 0.48 | 65.40 ± 2.48 |
8 | 20 | 3 | 1 | 0.33 | 0 | 1 | 0.11 | 0 | 0.33 | 0 | 0 | 18.35 ± 0.47 | 66.48 ± 1.88 |
8 | 25 | 3 | 1 | 0.67 | 0 | 1 | 0.44 | 0 | 0.67 | 0 | 0 | 19.05 ± 0.49 | 69.02 ± 2.32 |
8 | 30 | 3 | 1 | 1 | 0 | 1 | 1 | 0 | 1 | 0 | 0 | 19.49 ± 0.55 | 70.61 ± 2.84 |
5 | 0 | 4.5 | −1 | −1 | 1 | 1 | 1 | 1 | 1 | −1 | −1 | 11.4 ± 0.41 | 27.54 ± 1.84 |
5 | 5 | 4.5 | −1 | −0.67 | 1 | 1 | 0.44 | 1 | 0.67 | −0.67 | −1 | 18.04 ± 0.32 | 43.57 ± 2.20 |
5 | 10 | 4.5 | −1 | −0.33 | 1 | 1 | 0.11 | 1 | 0.33 | −0.33 | −1 | 18.69 ± 0.28 | 45.14 ± 1.48 |
5 | 15 | 4.5 | −1 | 0 | 1 | 1 | 0 | 1 | 0 | 0 | −1 | 19.55 ± 0.27 | 47.22 ± 1.52 |
5 | 20 | 4.5 | −1 | 0.33 | 1 | 1 | 0.11 | 1 | −0.33 | 0.33 | −1 | 20.02 ± 0.28 | 48.36 ± 2.16 |
5 | 25 | 4.5 | −1 | 0.67 | 1 | 1 | 0.44 | 1 | −0.67 | 0.67 | −1 | 20.58 ± 0.28 | 49.71 ± 2.35 |
5 | 30 | 4.5 | −1 | 1 | 1 | 1 | 1 | 1 | −1 | 1 | −1 | 21.1 ± 0.32 | 50.97 ± 2.11 |
6 | 0 | 4.5 | −0.33 | −1 | 1 | 0.11 | 1 | 1 | 0.33 | −1 | −0.33 | 11.4 ± 0.41 | 27.54 ± 1.84 |
6 | 5 | 4.5 | −0.33 | −0.67 | 1 | 0.11 | 0.44 | 1 | 0.22 | −0.67 | −0.33 | 19.67 ± 0.59 | 47.51 ± 2.38 |
6 | 10 | 4.5 | −0.33 | −0.33 | 1 | 0.11 | 0.11 | 1 | 0.11 | −0.33 | −0.33 | 20.55 ± 0.55 | 49.64 ± 2.17 |
6 | 15 | 4.5 | −0.33 | 0 | 1 | 0.11 | 0 | 1 | 0 | 0 | −0.33 | 21.99 ± 0.52 | 53.11 ± 2.54 |
6 | 20 | 4.5 | −0.33 | 0.33 | 1 | 0.11 | 0.11 | 1 | −0.11 | 0.33 | −0.33 | 23.32 ± 0.51 | 56.33 ± 3.01 |
6 | 25 | 4.5 | −0.33 | 0.67 | 1 | 0.11 | 0.44 | 1 | −0.22 | 0.67 | −0.33 | 23.83 ± 0.52 | 57.56 ± 2.97 |
6 | 30 | 4.5 | −0.33 | 1 | 1 | 0.11 | 1 | 1 | −0.33 | 1 | −0.33 | 24.02 ± 0.57 | 58.02 ± 1.53 |
7 | 0 | 4.5 | 0.33 | −1 | 1 | 0.11 | 1 | 1 | −0.33 | −1 | 0.33 | 11.4 ± 0.41 | 27.54 ± 1.84 |
7 | 5 | 4.5 | 0.33 | −0.67 | 1 | 0.11 | 0.44 | 1 | −0.22 | −0.67 | 0.33 | 27.19 ± 0.61 | 65.68 ± 2.56 |
7 | 10 | 4.5 | 0.33 | −0.33 | 1 | 0.11 | 0.11 | 1 | −0.11 | −0.33 | 0.33 | 27.48 ± 0.56 | 66.38 ± 3.45 |
7 | 15 | 4.5 | 0.33 | 0 | 1 | 0.11 | 0 | 1 | 0 | 0 | 0.33 | 28.15 ± 0.53 | 67.99 ± 1.48 |
7 | 20 | 4.5 | 0.33 | 0.33 | 1 | 0.11 | 0.11 | 1 | 0.11 | 0.33 | 0.33 | 28.98 ± 0.41 | 70.00 ± 2.52 |
7 | 25 | 4.5 | 0.33 | 0.67 | 1 | 0.11 | 0.44 | 1 | 0.22 | 0.67 | 0.33 | 29.64 ± 0.49 | 71.59 ± 1.94 |
7 | 30 | 4.5 | 0.33 | 1 | 1 | 0.11 | 1 | 1 | 0.33 | 1 | 0.33 | 30.02 ± 0.40 | 72.51 ± 2.64 |
8 | 0 | 4.5 | 1 | −1 | 1 | 1 | 1 | 1 | −1 | −1 | 1 | 11.4 ± 0.41 | 27.54 ± 1.84 |
8 | 5 | 4.5 | 1 | −0.67 | 1 | 1 | 0.44 | 1 | −0.67 | −0.67 | 1 | 25.09 ± 1.21 | 60.60 ± 2.35 |
8 | 10 | 4.5 | 1 | −0.33 | 1 | 1 | 0.11 | 1 | −0.33 | −0.33 | 1 | 27.58 ± 0.37 | 66.62 ± 3.64 |
8 | 15 | 4.5 | 1 | 0 | 1 | 1 | 0 | 1 | 0 | 0 | 1 | 30.58 ± 1.11 | 73.86 ± 2.45 |
8 | 20 | 4.5 | 1 | 0.33 | 1 | 1 | 0.11 | 1 | 0.33 | 0.33 | 1 | 31.98 ± 0.72 | 77.25 ± 1.98 |
8 | 25 | 4.5 | 1 | 0.67 | 1 | 1 | 0.44 | 1 | 0.67 | 0.67 | 1 | 32.58 ± 1.08 | 78.70 ± 2.23 |
8 | 30 | 4.5 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 32.69 ± 0.59 | 78.96 ± 2.18 |