. 2020 Dec 24;72:105423. doi: 10.1016/j.ultsonch.2020.105423

Table 1.

FCCD design matrix of the PUAE process parameters and resultant responses.

Std Run	S/S Ratio (g/100 mL)	Power (W)	Duty Cycle (%)	Time (Min.)	Yield(g/g)	TPC (mg GAE/g DW)	TFC (mg QE/g DW)	AOX (mg GAE/g DW)	TAC (mg Cyn-3-glc eq/100 g DW)	BI
1.	2.00	70.00	20.00	1.00	0.33 ± 0.04^de	80.69 ± 3.8^lm	18.51 ± 2.7ⁱ	122.94 ± 7.8^bcde	7.02 ± 1.00 ^h	74.86 ± 3.4^a
2.	10.00	70.00	20.00	1.00	0.25 ± 0.01^e	75.58 ± 4.2^m	9.31 ± 1.0^j	85.66 ± 6.1^e	7.39 ± 0.05 ^h	43.96 ± 2.4^fgh
3.	2.00	210.00	20.00	1.00	0.43 ± 0.02^abcd	131.78 ± 6.0^efgh	27.38 ± 1.4^defg	167.36 ± 8.6^ab	15.32 ± 2.43 ^g	70.89 ± 4.4^ab
4.	10.00	210.00	20.00	1.00	0.35 ± 0.01^bcde	111.46 ± 4.7^hijk	17.56 ± 3.0ⁱ	120.14 ± 7.3^cde	14.24 ± 0.27 ^g	43.46 ± 1.8^gh
5.	2.00	70.00	80.00	1.00	0.41 ± 0.00^abcd	120.52 ± 6.4^hij	25.97 ± 0.5^efgh	142.56 ± 4.3^abcd	15.70 ± 0.94 ^g	73.27 ± 5.2^ab
6.	10.00	70.00	80.00	1.00	0.33 ± 0.02^de	106.32 ± 3.1^ijk	17.66 ± 2.9ⁱ	134.13 ± 16.0^abcd	15.01 ± 0.17 ^g	42.01 ± 1.4^ghi
7.	2.00	210.00	80.00	1.00	0.43 ± 0.08^abcd	126.98 ± 2.4^fghi	28.26 ± 0.3^cdefg	144.31 ± 11.2^abcd	16.67 ± 0.33 ^fg	64.11 ± 3.3^bcd
8.	10.00	210.00	80.00	1.00	0.36 ± 0.02^bcde	101.27 ± 7.1^jkl	20.86 ± 0.7^hi	129.61 ± 6.4^abcde	17.67 ± 0.28^cdefg	41.27 ± 2.4^ghi
9.	2.00	70.00	20.00	10.00	0.37 ± 0.05^bcd	111.49 ± 4.3^hijk	25.73 ± 2.7^fgh	135.98 ± 8.2^abcd	18.23 ± 0.49^bcdefg	66.09 ± 3.4^abc
10.	10.00	70.00	20.00	10.00	0.34 ± 0.03^cde	92.60 ± 3.9^klm	20.74 ± 1.9^hi	112.22 ± 8.0^de	17.56 ± 0.07^efg	50.42 ± 2.3^efg
11.	2.00	210.00	20.00	10.00	0.42 ± 0.09^abcd	162.05 ± 1.2^abcd	33.80 ± 0.1^abc	172.05 ± 10.5^a	23.85 ± 1.69^a	56.72 ± 3.3^cde
12.	10.00	210.00	20.00	10.00	0.40 ± 0.09^bcd	131.34 ± 5.2^efgh	27.95 ± 2.2^defg	150.06 ± 12.1^abcd	22.67 ± 0.05^abcd	41.47 ± 1.5^ghi
13.	2.00	70.00	80.00	10.00	0.46 ± 0.01^ab	176.66 ± 0.7^ab	34.99 ± 0.4^ab	167.31 ± 3.1^ab	21.59 ± 0.63^abcdef	53.52 ± 3.3^ef
14.	10.00	70.00	80.00	10.00	0.43 ± 0.05^abcd	152.74 ± 1.8^bcde	30.50 ± 0.1^bcdef	163.98 ± 11.1^abc	22.24 ± 0.43^abcde	41.43 ± 2.4^ghi
15.	2.00	210.00	80.00	10.00	0.44 ± 0.07^abcd	182.66 ± 0.4^a	37.07 ± 0.0^a	163.55 ± 11.7^abc	22.71 ± 1.39^abc	29.64 ± 1.4^jk
16.	10.00	210.00	80.00	10.00	0.38 ± 0.04^bcd	151.88 ± 3.9^cde	32.33 ± 1.4^abcd	161.69 ± 8.4^abc	21.17 ± 0.62^abcdef	20.28 ± 1.2 ^k
17.	2.00	140.00	50.00	5.50	0.52 ± 0.10^a	171.72 ± 1.0^abc	35.43 ± 1.2^ab	165.93 ± 1.2^abc	23.60 ± 0.34^a	56.04 ± 4.3^de
18.	10.00	140.00	50.00	5.50	0.44 ± 0.01^abcd	147.65 ± 0.5^def	30.42 ± 1.9^bcdef	133.35 ± 1.2^abcd	21.24 ± 0.43^abcdef	40.47 ± 3.4^hi
19.	6.00	70.00	50.00	5.50	0.41 ± 0.02^abcd	120.18 ± 3.2^hij	27.43 ± 0.4^defg	122.61 ± 2.9^bcde	20.93 ± 0.02^abcdef	50.47 ± 4.2^efg
20.	6.00	210.00	50.00	5.50	0.45 ± 0.03^abcd	144.84 ± 1.8^defg	31.24 ± 1.2^bcdef	136.89 ± 2.0^abcd	21.98 ± 0.51^abcde	42.22 ± 3.3^ghi
21.	6.00	140.00	20.00	5.50	0.42 ± 0.01^abcd	122.54 ± 2.8^ghij	28.53 ± 0.7^cdefg	129.70 ± 0.7^abcde	21.40 ± 0.57^abcdef	42.14 ± 2.2^ghi
22.	6.00	140.00	80.00	5.50	0.45 ± 0.01^abc	152.44 ± 3.6^cde	32.36 ± 1.0^abcd	143.27 ± 0.1^abcd	21.69 ± 0.79^abcdef	30.45 ± 1.5^j
23.	6.00	140.00	50.00	1.00	0.37 ± 0.01^bcd	98.71 ± 4.7^jklm	24.43 ± 1.9^gh	114.26 ± 1.3^de	17.66 ± 0.47^defg	41.35 ± 3.4^ghi
24.	6.00	140.00	50.00	10.00	0.43 ± 0.04^abcd	146.14 ± 4.1^defg	33.14 ± 1.5^abcd	145.61 ± 0.0^abcd	24.84 ± 0.05^a	33.41 ± 2.3^ij
25.	6.00	140.00	50.00	5.50	0.44 ± 0.03^abcd	151.82 ± 3.6^cde	31.52 ± 1.5^abcde	138.04 ± 0.6^abcd	22.77 ± 0.65^ab	48.42 ± 4.2^efgh
26.	6.00	140.00	50.00	5.50	0.46 ± 0.02^ab	153.73 ± 1.3^bcde	31.26 ± 1.1^bcdef	137.64 ± 0.1^abcd	23.21 ± 0.28^ab	44.00 ± 2.4^fgh
27.	6.00	140.00	50.00	5.50	0.45 ± 0.01^abcd	156.83 ± 0.7^bcd	32.43 ± 0.2^abcd	143.78 ± 2.2^abcd	22.77 ± 0.25^ab	44.56 ± 3.3^fgh
28.	6.00	140.00	50.00	5.50	0.45 ± 0.02^abcd	149.80 ± 0.7^cdef	32.36 ± 0.2^abcd	137.28 ± 0.4^abcd	22.14 ± 0.09^bcde	42.61 ± 3.5^ghi
29.	6.00	140.00	50.00	5.50	0.45 ± 0.02^abcd	158.27 ± 0.7^bcd	31.93 ± 0.3^abcd	136.79 ± 0.4^abcd	22.51 ± 0.10^bcde	43.50 ± 2.1^gh
30.	6.00	140.00	50.00	5.50	0.44 ± 0.01^abcd	153.67 ± 0.8^bcde	31.85 ± 0.1^abcd	141.90 ± 0.5^abcd	23.60 ± 0.02^a	45.91 ± 3.4^fgh

Each parameter was analysed and calculated in five times and values are expressed as mean ± Std. deviation. In the column, the different small letters of alphabets signify that the mean values belong to distinct subsets at 95% confidence interval. TPC: total phenolics content, TFC: total flavonoids content AOX: antioxidant capacity, TAC: total anthocyanin content, and BI: browning index