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. 2021 Jan 1;77(Pt 1):13–21. doi: 10.1107/S2053230X20016829

Table 3. Data collection and processing.

Diffraction source BL41XU, SPring-8
Wavelength (Å) 1.0000
Temperature (K) 100
Detector PILATUS3 6M
Crystal-to-detector distance (mm) 250
Rotation range per image (°) 0.1
Total rotation range (°) 180
Exposure time per image (s) 0.1
Space group P212121
a, b, c (Å) 49.62, 56.28, 81.10
α, β, γ (°) 90, 90, 90
Mosaicity (°) 0.1
Resolution range (Å) 46.31–2.30 (2.36–2.30)
Total No. of reflections 135479 (8910)
No. of unique reflections 10568 (757)
Completeness (%) 99.8 (97.4)
Multiplicity 12.8 (11.8)
I/σ(I)〉 21.8 (2.1)
R r.i.m. 0.074 (1.284)
Overall B factor from Wilson plot (Å2) 61.55