Table 1.
Cpd. | R | X | IC50 [nM] 1 | |
---|---|---|---|---|
E. coli | ||||
DNA Gyrase | Topoisomerase IV | |||
3a | H | 450 ± 180 | 1000 ± 150 | |
3b | OBn | 3300 ± 1500 | >10,000 | |
7a | H | 92 ± 10 | 2500 ± 1300 | |
7b | H | 130 ± 10 | 3100 ± 0 | |
11a 2 | H | 130 ± 30 | >10,000 | |
11b 3 | OBn | 14 ± 9 | 2500 ± 1100 | |
1a 4 | 13 ± 0 | 500 ± 280 | ||
1b 5 | <10 | 350 ± 50 | ||
CP 6 | 120 ± 20 | 5400 ± 2100 | ||
NB 7 | 170 ± 20 | 11,000 ± 2000 |
1 Concentration of compound (mean ±SD, in nM) that inhibits the enzyme activity by 50%; 2, 3 Compounds 11a and 11b were obtained as hydrochloride salts; 4, 5 1a and 1b, GyrB and ParE inhibitors; 6 CP, ciprofloxacin; 7 NB, novobiocin.