Table 9.
Limit of detection (LOD) and quantification (LOQ) from serum and milk samples and their corresponding recovery of ZEN, DON, and their metabolites.
| Serum | Colostrum/Milk | |||||
|---|---|---|---|---|---|---|
| Recovery ± SD | LOD | LOQ | Recovery ± SD | LOD | LOQ | |
| ZEN | 105 ± 4 | 0.01 | 0.03 | 112 ± 2 | 0.04 | 0.12 |
| α-ZEL | 100 ± 4 | 0.02 | 0.08 | 94 ± 2 | 0.04 | 0.14 |
| β-ZEL | 92 ± 4 | 0.08 | 0.26 | 90 ± 4 | 0.10 | 0.34 |
| ZAN | 85 ± 4 | 0.07 | 0.24 | 102 ± 9 | 0.22 | 0.73 |
| α-ZAL | 97 ± 3 | 0.31 | 1.03 | 98 ± 3 | 0.26 | 0.88 |
| β-ZAL | 102 ± 4 | 0.69 | 2.31 | 103 ± 2 | 0.81 | 2.71 |
| DON | 108 ± 4 | 0.09 | 0.28 | 111 ± 3 | 0.11 | 0.36 |
| de-DON | 102 ± 7 | 0.08 | 0.26 | 108 ± 8 | 0.20 | 0.13 |
| ZEN | 105 ± 4 | 0.01 | 0.03 | 112 ± 2 | 0.04 | 0.12 |