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. 2021 Jan 18;26(2):483. doi: 10.3390/molecules26020483

Scheme 25.

Scheme 25

Synthesis of 4H-thieno[2,3-c]benzopyran-4-one (88). Reagents and conditions: 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU), 1,4-dioxane, 60 °C, 12 h, N2, 95% yield.