Table 2.
Optimized mass parameters for sivelestat, XW-IMP-A and the internal standards.
Analyte | MRM (m/z) | Dwell time (ms) | DP (V) | CE (eV) | EP (V) | CXP (V) |
---|---|---|---|---|---|---|
Sivelestat | 435.1→360.0 | 100 | 50 | 22 | 10 | 11 |
XWCl | 469.0→394.0 | 100 | 50 | 22 | 10 | 11 |
XW-IMP-A | 351.0→276.0 | 100 | 50 | 22 | 10 | 11 |
XWCl-A | 384.9→310.0 | 100 | 50 | 22 | 10 | 11 |
Note: DP: declustering potential, CE: collision energy, EP: entrance potential, CXP: collision cell exit potential, ms: millisecond.