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. 2021 Jan 5;77(Pt 1):42–53. doi: 10.1107/S205327332001548X

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© Vladimir M. Kaganer et al. 2021

This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

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The measured GISAXS intensities (three left-hand columns) and Monte Carlo simulations (right-most column) for (a)–(d) sample 1, (e)–(h) sample 2 and (i)–(l) sample 3. The measurements are performed for different mean orientation angles ψ of the side facets of the NWs with respect to the X-ray beam, namely from 0° to 90° in steps of 5°. For clarity, these measurements are presented in three different panels (from 0° to 30°, from 30° to 60° and from 60° to 90°). The intensities are plotted as versus q _x to highlight deviations from Porod’s law. The curves calculated at ψ = 0° for each sample are repeated as blue curves in the left-most column, for direct comparison of the calculated and measured curves.

Inline graphic — The measured GISAXS intensities (three left-hand columns) and Monte Carlo simulations (right-most column) for (a)–(d) sample 1, (e)–(h) sample 2 and (i)–(l) sample 3. The measurements are performed for different mean orientation angles ψ of the side facets of the NWs with respect to the X-ray beam, namely from 0° to 90° in steps of 5°. For clarity, these measurements are presented in three different panels (from 0° to 30°, from 30° to 60° and from 60° to 90°). The intensities are plotted as versus q _x to highlight deviations from Porod’s law. The curves calculated at ψ = 0° for each sample are repeated as blue curves in the left-most column, for direct comparison of the calculated and measured curves.