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Structural and morphological characterizations. (a) Synthesis route and building blocks of TTCOF-Mn and its top and side viewed structure. (b) Simulated (blue) and experimental PXRD patterns of TTCOF-Mn (red) and TTCOF-2H (black). (c) CO2 adsorption–desorption isotherms of TTCOF-Mn (red) and TTCOF-2H (black). (d) TEM image (scale bar: 50 nm) and (e) HRTEM image (scale bar: 5 nm) of TTCOF-Mn; the inset is the AA-stacking mode of the 2D TTCOF-Mn structure.
