Table 1.
Instrument Parameters | |
---|---|
Column | HP-5MS UI (30 m × 0.250 mm × 0.25 μm) |
Carrier gas flow | He @ 1.00 mL/min (constant flow) |
Inlet temperature | 250°C |
Oven program | Ramp 1: 40°C to 170°C @ 10°C/min; hold 2 min; Ramp 2: 8°C/min to 250°C; Ramp 3: 25°C/min to 320°C; hold 5 min. |
Injection volume | 250 µL, split (20:1) |
Transfer line temperature | 290°C |
MS source | Single quadrupole, EI @ 250°C |
Solvent delay | 1.00 min |
MS acquisition range | 30–450 amu from 1 min to 32.80 min |