Table 10.
Experimental13C chemical shift in ppm of Br-1 to Br-8.
| Br -1 | Br -2 | Br -3 | Br -4 | Br -5 | Br -6 | Br -7 | Br -8 | |
|---|---|---|---|---|---|---|---|---|
| C1 | 175.00 | 175.60 | 175.13 | 175.08 | 175.09 | 175.08 | 175.12 | 175.11 |
| C2 | 148.29 | 147.87 | 147.87 | 147.28 | 147.30 | 147.37 | 147.37 | 147.30 |
| C3 | 129.96 | 130.38 | 129.87 | 129.81 | 129.85 | 129.84 | 129.85 | 129.85 |
| C4 | 179.94 | 180.35 | 179.85 | 179.80 | 179.84 | 179.83 | 179.86 | 179.86 |
| C5 | 125.96 | 126.50 | 126.04 | 126.52 | 126.03 | 126.54 | 126.02 | 126.57 |
| C6 | 133.00 | 133.00 | 132.54 | 132.49 | 132.51 | 132.51 | 132.56 | 132.52 |
| C7 | 134.75 | 135.26 | 134.80 | 134.77 | 134.81 | 134.78 | 134.80 | 134.81 |
| C8 | 126.50 | 127.04 | 126.57 | 126.01 | 126.55 | 126.01 | 126.55 | 126.03 |
| C9 | 131.82 | 132.24 | 131.76 | 131.74 | 131.76 | 131.75 | 131.77 | 131.77 |
| C10 | 131.82 | 132.24 | 131.76 | 131.74 | 131.76 | 131.75 | 131.77 | 131.77 |
| a | 32.79 | 16.78 | 10.82 | 13.65 | 13.85 | 13.79 | 13.87 | 13.90 |
| b | - | - | 23.87 | 19.26 | 21.80 | 21.95 | 21.95 | 22.04 |
| c | - | - | - | - | 28.22 | 30.26 | 25.95 | 31.16 |
| d | - | - | - | - | - | 25.65 | 28.31 | 28.62 |
| e | - | - | - | - | - | - | 31.12 | 28.58 |
| f | - | - | - | - | - | - | - | 25.98 |
| g | - | - | - | 32.65 | 30.24 | 30.47 | 30.50 | 30.51 |
| h | - | 39.61 | 45.67 | 43.82 | 44.04 | 44.08 | 44.08 | 44.05 |