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. 2021 Feb 3;11:2940. doi: 10.1038/s41598-021-82585-7

Table 2.

The resonance assignments of 1H and 13C based on the NMR analysis of the novel MAGE.

Position 1H NMR δ (ppm) 13C NMR δ (ppm)
Isomer α Isomer β keto Isomer α Isomer β keto
6 2.71 2.76 2.58 48.24 47.87 47.93
2-NH 7.70 7.64 7.77
7 168.51 168.64
8 1.8311 1.829 1.828 22.70
1′ 2.85 2.94; 2.97 2.58 53.120 51.22 48.00
2′ 100.54 102.30 205.74
3′ 3.90 3.88 80.05 82.94
4′ 3.82 3.80 76.57 77.81
5′ 3.72 3.95 80.04 75.18
6′

3.67

3.403

3.63; 3.45 68.35 66.27
1″ 4.67 (br)

3.68

J = 3.7 Hz

4.65

J = 4.12 Hz

99.11 99.17 98.89
5″ 3.08 70.98 71.07 70.87
6″

3.446

3.516

60.52 60.46 60.33