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. 2021 Jan 21;6(4):3278–3290. doi: 10.1021/acsomega.0c05765

Table 2. Temperature and Mass Loss of Each Degradation Stage of Unprocessed PHBV, Processed PHBV and its Formulations with PLAP, Residual Mass Fraction at 500 °C, and the PLAP Mass Fraction Determined by TGA Analysis.

1st stage
2nd stage
wPLAP Tonset (°C) Tmax. (°C) mass loss (%) Tonset (°C) Tmax. (°C) mass loss (%) R500°C (%) wPLAP,realc
0.00a 240 300 100       0  
0.00 220 295 100       0  
0.10 205 260 92 285 345 8 0 0.09
0.20 200 255 85 280 350 14 1 0.17
0.30 200 255 75 280 350 23 2 0.28
1.00b 190 280 11 300 385 87 2  
a

Unprocessed PHBV.

b

Unprocessed PLAP.

c

wPLAP,real = {[(mass loss2ndstage/87) × 100] + residue}/100.