Bruker Kappa Mach3 APEXII diffractometer	8316 independent reflections
Radiation source: microfocus X-ray tube	5593 reflections with I > 2σ(I)
Incoatec Helios mirrors monochromator	Rint = 0.080
Detector resolution: 66.67 pixels mm-1	θmax = 34.3°, θmin = 1.4°
φ– and ω–scans	h = −13→13
Absorption correction: gaussian (SADABS; Bruker, 2012)	k = −44→43
Tmin = 0.989, Tmax = 0.996	l = −14→14
64252 measured reflections