Table 1. Data collection and processing.
Values in parentheses are for the outer shell.
| CRABPI-L29C–MYR | CRABPI-L29C–DC645 | CRABPII–DC479 | CRABPII–DC645 | |
|---|---|---|---|---|
| PDB code | 7a9y | 7a9z | 7aa0 | 7aa1 |
| Diffraction source | I03, DLS | I04, DLS | I03, DLS | I24, DLS |
| Wavelength (Å) | 0.9763 | 0.9763 | 0.9763 | 0.9763 |
| Temperature (K) | 100 | 100 | 100 | 100 |
| Detector | PILATUS 6M | PILATUS 6M | PILATUS 6M | PILATUS 6M |
| Crystal-to-detector distance (mm) | 213.39 | 385.58 | 321.83 | 186.39 |
| Rotation range per image (°) | 0.1 | 0.1 | 0.1 | 0.1 |
| Total rotation range (°) | 200 | 360 | 200 | 180 |
| Exposure time per image (s) | 0.05 | 0.05 | 0.05 | 0.1 |
| Space group | I222 | P3121 | P21 | P213 |
| a, b, c (Å) | 36.89, 109.98, 170.34 | 127.54, 127.54, 52.16 | 39.56, 49.92, 67.37 | 78.56, 78.56, 78.56 |
| α, β, γ (°) | 90.0, 90.0, 90.0 | 90.00, 90.00, 120.00, | 90.00, 96.04, 90.00 | 90.0, 90.0, 90.0 |
| Mosaicity (°) | 0.00 | 0.00 | 0.70 | 0.00 |
| Resolution range (Å) | 36.05–1.64 | 110.46–2.41 | 49.92–1.82 | 45.36–1.71 |
| Total No. of reflections | 81769 | 366266 | 80669 | 326013 |
| No. of unique reflections | 43112 | 19102 | 23023 | 17775 |
| Completeness (%) | 99.9 (100) | 99.9 (99.3) | 97.6 (96.8) | 100.0 (100.0) |
| Multiplicity | 1.9 (1.9) | 19.2 (16.8) | 3.5 (3.7) | 18.3 (18.3) |
| CC1/2 | 0.998 (0.480) | 0.994 (0.398) | 0.996 (0.486) | 0.999 (0.548) |
| 〈I/σ(I)〉 | 9.8 (1.1)† | 7.1 (0.5)† | 10.4 (1.6)† | 18.8 (1.2)† |
| R p.i.m. | 0.029 (0.559) | 0.088 (1.624) | 0.059 (0.504) | 0.019 (0.554) |
| Overall B factor from Wilson plot (Å2) | 26.42 | 47.34 | 26.78 | 31.81 |
†
The resolution cutoff was automatically selected based on CC1/2 rather than outer shell I/σ(I).