Table 4:
Position | δc, type | δH, mult (J in Hz) | position | δc, type | δH, mult (J in Hz) |
---|---|---|---|---|---|
1 | 146.6, C | - | 8 | 197.3, C | - |
2 | 137.2, C | - | 9 | 158.3, C | - |
3 | 149.3, C | - | 10 | 125.0, CH | 6.56, d (3.4) |
4 | 108.2, CH | 6.60, s | 10a | 43.8, CH | 4.24, dd (3.4, 2.8) |
4a | 135.9, C | - | 10b | 158.3, C | - |
5 | 30.8, CH2 | 2.85, m | 10c | 118.7, C | - |
6 | 40.8, CH2 | 2.64, m | 11 | 61.2, CH3 | 4.04, s |
7 | 194.8, C | - | 12 | 56.5, CH3 | 3.95, s |
7a | 133.6, C | - | 13 | 57.0, CH3 | 3.68, s |
7b | 48.6, CH | 3.90, d (2.8) | 2-OH | 5.52, s |