Table 3.

Crystallite and particle size as determined by PXRD and TEM, respectively.

sample	stoichiometry	PXRD		TEM
		size (nm)	strain (%)	mean size (s.d.) (nm)
A	K0Cu[Fe(CN)6]0.59	49.5	9.45	55 (16)
B	K0.23Cu[Fe(CN)6]0.49	23.6	42.70	30 (9)
C	K0.24Cu[Fe(CN)6]0.69	33.0	36.27	30 (8)
D	K1.10Cu[Fe(CN)6]0.73	14.5	61.59	20 (4)
E	KFeFe(CN)6	25.3	134.31	15 (3)
F	K0.25Fe[Fe(CN)6]0.79	16.4	29.41	20 (5)
G	K0.18Cu[Fe(CN)6]0.69	53.3	25.66	80 (40)
H	K0.74FeIII[FeIII/II(CN)6]0.67	192.4	33.60	800 (120)
I	K0.10Cu[Fe(CN)6]0.68	37.3	27.69	48 (18)
J	K1.51Cu[Fe(CN)6]0.79	11.2	98.08	a
K	K0.86Cu[Fe(CN)6]0.72	31.9	54.40	24 (5)
L	K1.86Mn[Fe(CN)6]0.97	116.1	11.06	71 (49)

^aIndividual particle size cannot be determined owing to agglomeration.