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. 2021 Feb 8;6(7):4511–4526. doi: 10.1021/acsomega.0c06070

Table 2. Overview of Current Preparation/Synthesis Methods for Nanocellulosic Materials.

type of nanocellulosic preparation/synthesis methods refs
CNF/CNCs acid hydrolysis of cellulose pulp in the presence of either mineral or organic acid (97) and (98)
  enzymatic hydrolysis employing the cellulose enzyme. Although an environmentally friendly route, it is very expensive  
  subcritical water extraction. Also, an environmentally friendly method but nanocellulosics obtained from this method demonstrate instability in suspension  
  transition metals catalysis such as Fe(III), Co(II), etc., have been used for effective hydrolysis for obtaining nanocellulosic materials from cellulose pulp, thereby reducing the use of acids  
  ionic liquid hydrolysis methodology. Notwithstanding the noteworthy efficiency in using this process for NC production, they, however, come with drawbacks such as toxicity, high-cost implications, and high chemical footprints  
  deep eutectic solvents hydrolysis. Similar to ionic liquids; however, it eliminates some noted drawbacks associated with the use of ionic liquids for cellulose pulp hydrolysis which includes lower-cost implications and simplicity  
BNC fermentation process. However, it comes with challenges such as the long cultivation period (99101)
  bioreactor process