Table 2.
Position | Compound 1 | |
---|---|---|
δC, Type | δH (J in Hz) | |
1 | 56.0, C | |
2 | 66.0, CH | 4.13, dd (10.4, 4.8) |
3 | 69.8, CH | 5.17, dd (4.8, 2.8) |
4 | 51.0, CH | 3.31, t (2.8) |
5 | 48.0, CH | 3.55, t (2.8) |
6 | 53.8, CH | 3.70, d (2.8) |
7a | 64.8, CH2 | 4.54, d (12.0) |
7b | 64.8, CH2 | 4.42, d (12.0) |
1’ | 129.4, C | |
2’,6’ | 129.9, CH | 8.05, m |
3’,5’ | 128.7, CH | 7.47, m |
4’ | 133.7, CH | 7.59, m |
C=O | 166.1, C | |
C=O | 170.0, C | |
2-OH | 2.69, d (10.4) | |
Me | 20.6, CH3 | 1.89, s |