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. 2021 Feb 3;14(4):706. doi: 10.3390/ma14040706

Table 1.

MNP parameters and the corresponding characterization techniques. Adapted from [15,16]. See list of acronyms at the end of the document.

Structural Properties
Particle, core and aggregate size TEM, XRD, DLS, NTA, SAXS, HRTEM, SEM, AFM, EXAFS, FMR, DCS, MALDI, NMR, TRPS, EPLS, magnetic susceptibility
Morphology TEM, HRTEM, AFM, EPLS, FMR, 3D-tomography
Elemental-chemical composition XRD, XPS, ICP-MS, ICP-OES, SEM-EDX, NMR, MFM, LEIS
Crystallinity XRD, EXAFS, HRTEM, electron diffraction, STEM
Structural defects HRTEM, EBSD
Chemical state–oxidation state XAS, EELS, XPS, Mössbauer
Ligand-binding, surface composition XPS, FTIR, NMR, SIMS, FMR, TGA, SANS
Colloidal Properties
Hydrodynamic and aggregate size NTA, DLS, DCS, UV-vis, SEM, TEM, Cryo-TEM
3D visualization 3D-tomography, AFM, SEM
MNP charge Zeta potential, EPM
Element concentration ICP-MS, UV-vis, RMM-MEMS, PTA, DCS, TRPS
Magnetic Properties
Quasi-static magnetization properties SQUID, VSM, Mössbauer, MFM, FMR, XMCD,
Dynamical magnetization properties AC susceptometry and magnetometry, magnetorelaxometry, magnetic particle spectroscopy
Magnetic losses AC calorimetry, AC susceptometry and magnetometry