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. 2021 Feb 12;10(2):145. doi: 10.3390/biology10020145

Table 2.

13C NMR data (δ ppm) for compounds 1–4 and 7 *.

Pos. 1 ** 2 *** 3 ** 4 ** 7 ** Pos. 1 ** 2 *** 3 ** 4 ** 7 **
1 93.95 94.03 93.82 93.76 93.83 3″ 69.45 69.22 69.46 69.39 68.84
3 141.14 141.75 141.14 141.12 140.97 4″ 71.05 70.70 71.07 70.90 74.15
4 102.06 102.46 101.95 101.80 102.09 5″ 66.89 65.89 66.88 66.65 66.86
5 35.78 35.80 35.81 35.75 35.93 6″ 16.53 17.62 16.54 16.35 16.54
6 83.74 83.21 83.61 83.47 82.77 1‴ 134.00 134.11 133.97 134.07 134.32
7 58.02 57.56 58.14 58.07 58.13 2‴–6‴ 128.01–130.45 129.01–131.26 128.00–130.43 128.04–130.46 127.95–130.26
8 65.08 66.62 65.21 65.19 65.25 7‴ 146.28 146.07 146.26 146.04 145.39
9 41.85 42.14 41.92 41.87 41.91 8‴ 116.50 117.41 116.51 116.47 117.42
10 60.17 59.22 60.07 60.01 60.06 9‴ 165.93 165.75 165.92 165.89 166.98
1′ 98.45 98.71 98.36 98.32 98.32 1″″ 134.00 - 133.97 - -
2′ 73.35 73.70 73.44 73.42 73.42 2″″–6″″ 128.01–130.45 - 128.00–130.43 - -
3′ 76.02 76.51 76.28 76.27 76.25 7″″ 146.07 - 146.05 - -
4′ 70.06 70.26 70.37 70.37 70.35 8″″ 116.50 - 116.51 - -
5′ 74.36 74.22 77.22 77.22 77.19 9″″ 166.31 - 166.30 - -
6′ 62.74 63.27 61.58 61.55 61.52 Acetyl: 6′ 19.54, 171.40 20.94, 170.72 - -
1″ 96.41 96.11 96.41 96.28 99.06 2″ 19.48, 170.32 21.07, 170.23 19.49, 170.31 19.37, 170.30 -
2″ 69.92 69.55 70.11 69.92 71.05 4″ - 21.04, 170.06 - 19.39, 170.53 -

* Assignments based on DEPT135, COSY, HSQC, HMBC, H2BC, NOESY experiments and comparison with reported data. ** Spectra measured in CD3OD. *** Spectra measured in DMSO d6.