Table 2. The Actual Metal Loadings of Pt and Rh of PtxRhy@HMSNs by ICP-OES.
| metal loadings (wt %) |
||||
|---|---|---|---|---|
| samplesa | nominal Pt/Rh | Pt/Rh by ICP-OES | Pt | Rh |
| Pt@HMSNs | N/A | N/A | 3.8 | N/A |
| Pt11.1Rh1@HMSNs | 3/1 | 11.1/1 | 5.9 | 0.28 |
| Pt2.5Rh1@HMSNs | 1/1 | 2.5/1 | 1.7 | 0.35 |
| Pt0.77Rh1@HMSNs | 1/3 | 0.77/1 | 1.2 | 0.82 |
| Rh@HMSNs | N/A | N/A | N/A | 1.6 |
All materials were calcined at 500 °C and subsequently reduced at 200 °C.