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. Author manuscript; available in PMC: 2021 Apr 6.
Published in final edited form as: Inorg Chem. 2020 Mar 20;59(7):5218–5230. doi: 10.1021/acs.inorgchem.0c00523

Table 1.

Instrumental Properties and Sample Requirements for the FIRMS and INS Experiments in This Study

feature approximate energy range used (cm−1) magnet used temperatures (K) amount of the sample used location
far-IR Bruker Vertex 80v FT-IR spectrometer from 20 to 700 17 T ∼4.6 5–10 mg of singlecrystals coated with eicosane
5–10 mg of powders mixed in eicosane		 National High Magnetic Field Laboratory (Maglab or NHMFL)
INS by DCS78 direct geometry51 with a monochromic incident neutron beam from ∼12 to ∼150 10 T 1.7 2.3 g packed in Hefilled aluminum can NIST Center for Neutron Research (NCNR)
INS by VISION79 indirect geometry51 with a white incident neutron beam (of all energies) from ∼10 to 20 (depending on the temperatures) to ∼4000 no magnet 5, 25, 50, 75, 100 2.3 g (same sample as that used in DCS) Spallation Neutron Source (SNS), Oak Ridge National Laboratory (ORNL)