Table 2. Hydrogen bonds in the basic structure.
The acceptor molecules are related to the donor molecule by the given symmetry operations. Since the positions of the H atoms were not refined, no esds are given.
| D—H⋯A | Acceptor symmetry | Occ. | D⋯H (Å) | H⋯A (Å) | D⋯A (Å) | D—H⋯A (°) |
|---|---|---|---|---|---|---|
| Inside I half-layer | ||||||
| O3—H⋯O5 | t(½, −½, 0) | ½ | 0.88 | 1.86 | 2.7316 (11) | 169 |
| O3—H⋯O6 | t(0,−1,0) | ½ | 0.84 | 2.12 | 2.9274 (9) | 163 |
| O4—H⋯O6 | t(0, −1, 0) | ½ | 0.88 | 2.04 | 2.9029 (10) | 171 |
| O5—H⋯O3 | t(−½, ½, 0) | ½ | 0.86 | 2.08 | 2.7316 (11) | 132 |
| O6—H⋯O2 | t(−½, ½, 0) | 1 | 0.87 | 2.20 | 3.0030 (10) | 154 |
| Across I half-layers | ||||||
| O4—H⋯O4 | 2 0, y, ½ | ½ | 0.85 | 1.98 | 2.8111 (11) | 165 |
| O5—H⋯O5 | 2 0, y, ½ | ½ | 0.86 | 1.82 | 2.6816 (11) | 175 |