Table 1. Parameters used for the XSA experiments with the MetalJet X-ray source.

Source	Liquid metal jet, 160 kV/1.56 mA (250 W), effective focus 20 × 20 µm
Optics (primary beam)	Polycapillary lens (f 2 = 900 mm, δ = 0.26°); exit beam cross section defined by pinholes with diameters 0.2 and 2.0 mm
Optics (diffracted beam)	Equatorial Soller slit (δ = 0.15°) + 1.0 mm entrance slit
Detector	Ge semiconductor detector (Canberra model GL0110); resolution: 160 eV at 10 keV and 420 eV at 100 keV
XSA mode	Symmetrical Ψ mode (ψ = −63°…63°), Δ(sin2ψ) = 0.05
Diffraction angle	2θ = 16.3°
Integration time	300 s (∅ = 2 mm), 3600 s (∅ = 0.2 mm)
Calibration measurement	Stress-free W powder, applied at the measuring point and analyzed under identical conditions
Data evaluation	MATLAB-based software package EDDIDAT (Apel et al., 2020 ▸)