Table 2.
Accuracy and precision results
Analyte | Nominal concentration (pg/mL) | Accuracy | Precision | |||||
---|---|---|---|---|---|---|---|---|
Day 1 RE (%) |
Day 2 RE (%) |
Day 3 RE (%) |
Between-run RE (%) |
Within-run CV (%) |
Between-run CV (%) |
|||
Kallidin | QC high | 750.0 | 1.1 | −1.5 | −2.1 | −0.8 | 3.1 | 3.2 |
QC mid | 125.0 | −0.9 | −4.6 | −1.6 | −2.4 | 3.3 | 3.6 | |
QC low | 7.8 | −8.0 | −8.5 | −11.1 | −9.2 | 8.9 | 8.9 | |
LLOQ | 3.9 | −14.6 | −9.0 | −12.7 | −12.1 | 10.9 | 10.9 | |
Bradykinin | QC high | 750.0 | 1.9 | −1.5 | −1.9 | −0.5 | 3.4 | 3.7 |
QC mid | 125.0 | −7.0 | −0.2 | −3.1 | −3.4 | 2.0 | 3.9 | |
QC low | 3.9 | 13.2 | 2.4 | −5.4 | 3.4 | 10.5 | 13.0 | |
LLOQ | 2.0 | 8.0 | −4.4 | −9.0 | −1.8 | 15.2 | 16.3 | |
Des-Arg(10)-kallidin | QC high | 750.0 | 2.2 | 1.9 | 1.4 | 1.8 | 3.0 | 3.0 |
QC mid | 125.0 | −5.7 | 0.8 | 2.8 | −0.7 | 2.7 | 5.1 | |
QC low | 3.9 | 2.7 | −11.6 | 9.7 | 0.3 | 11.2 | 14.7 | |
LLOQ | 2.0 | 5.4 | −5.7 | 3.8 | 1.2 | 18.4 | 18.4 | |
Des-Arg(9)-bradykinin | QC high | 750.0 | 2.7 | −4.5 | −0.5 | −0.8 | 2.5 | 4.3 |
QC mid | 125.0 | 3.2 | −5.6 | 5.5 | 1.1 | 2.4 | 6.2 | |
QC low | 3.9 | 1.6 | 14.5 | −5.9 | 3.4 | 7.7 | 12.1 | |
LLOQ | 2.0 | −1.6 | 11.9 | −17.1 | −2.3 | 14.7 | 19.8 | |
Bradykinin 2-9 | QC high | 750.0 | 4.7 | −0.3 | −0.2 | 1.4 | 2.3 | 3.5 |
QC mid | 125.0 | 2.4 | −4.3 | 6.5 | 1.5 | 4.8 | 6.9 | |
QC low | 15.6 | 13.8 | −0.2 | 9.9 | 7.8 | 9.8 | 11.0 | |
LLOQ | 7.8 | 13.5 | −3.9 | −4.2 | 1.8 | 15.4 | 17.0 | |
Bradykinin 1-7 | QC high | 750.0 | 1.1 | 1.9 | −1.9 | 0.4 | 2.3 | 2.8 |
QC mid | 125.0 | −1.6 | −1.6 | 0.2 | −1.0 | 3.0 | 3.0 | |
QC low | 3.9 | −4.5 | −2.7 | −6.5 | −4.6 | 7.5 | 7.5 | |
LLOQ | 1.9 | −4.5 | −3.5 | −16.9 | −8.3 | 13.6 | 14.6 | |
Bradykinin 1-5 | QC high | 750.0 | −2.9 | −1.0 | −5.2 | −3.0 | 2.7 | 3.2 |
QC mid | 125.0 | 0.1 | −4.4 | −0.4 | −1.6 | 5.3 | 5.4 | |
QC low | 31.1 | 9.5 | −5.7 | −4.6 | −0.2 | 12.3 | 13.9 | |
LLOQ | 15.6 | −6.8 | 1.9 | −8.6 | −4.5 | 11.9 | 12.2 |
CV coefficient of variation, LLOQ lower limit of quantification, QC quality control, RE relative error