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. 2021 Feb 25;12:654963. doi: 10.3389/fmicb.2021.654963

TABLE 2.

1H (600 MHz) and 13C (150 MHz) NMR data of compounds 1, 18, and 19 in DMSO-d6.

Position 1
18
19
δ C δ H (J in Hz)a δ C δ H (J in Hz) δ C δ H (J in Hz)
1 126.5, C 125.7, C 125.7, C
2 115.0, CH 6.88, d (1.8) 118.6, CH 6.75, d (2.0) 118.6, CH 6.74, d (2.0)
3 148.2, C 143.8, C 143.7, C
4 146.7, C 144.3, C 144.2, C
5 112.5, CH 6.96, d (8.3) 114.8, CH 6.71, d (8.0) 114.8, CH 6.71, d (8.0)
6 123.1, CH 6.82, dd (8.3, 1.8) 122.0, CH 6.60, dd (8.0, 2.0) 122.0, CH 6.59, dd (8.0, 1.9)
1′ 117.7, C 116.0, C 115.8, C
2′ 148.3, C 145.0, C 144.9, C
3′ 139.5, C 134.4, C 134.4, C
4′ 132.7, C 129.6, C 130.1, C
5′ 103.2, CH 6.46, s 106.5, CH 6.26, s 106.5, CH 6.24, s
6′ 153.2, C 148.2, C 148.1, C
1″ 138.2, C 128.2, C 128.2, C
2″ 128.7, CH 7.61, d (7.5) 130.0, CH 7.35, d (8.5) 116.6, CH 6.97, d (2.0)
3″ 128.4, CH 7.47, t (7.5) 114.9, CH 6.79, d (8.5) 144.7, C
4″ 127.3, CH 7.37, t (7.5) 156.2, C 144.2, C
5″ 128.4, CH 7.47, t (7.5) 114.9, CH 6.79, d (8.5) 115.3, CH 6.75, d (8.0)
6″ 128.7, CH 7.61, d (7.5) 130.0, CH 7.35, d (8.5) 119.9, CH 6.79, dd (8.0, 2.0)
1″′ 64.8, CH2 4.53, d (6.7)
2″′ 120.4, CH 5.47, t (6.7)
3″′ 136.9, C
4″′ 18.0, CH3 1.72, s
5″′ 25.5, CH3 1.76, s
3-OMe 55.5, CH3 3.73, s
3′-OMe 60.4, CH3 3.30, s
6′-OMe 55.7, CH3 3.67, s
2′-OH 8.68, s

ad, dd, s, t respectively means doublet, a doublet of doublets, singlet and triplet.