Table 3. FIC Values for HEDP, AEDP, ATMP, and New Hydroxybisphosphonate SIs for Calcite Scaleb.
calcite
scale |
||||||
---|---|---|---|---|---|---|
first blank | first
scale test |
second
scale test |
second blank | |||
SI (1000 ppm)c | time (min) | concn (ppm) | time (min) | concn (ppm) | time (min) | time (min) |
HEDP | 12 | 1 | 35 | 1 | 36 | 13 |
AEDP(28) | 6 | 20 | 22 | 20 | 21 | 8 |
ATMP(33) | 11 | 20 | 26 | 20 | 26 | 12 |
SI-1 | 17 | 2 | 26 | 2 | 26 | 17 |
SI-2 | 18 | 2 | 30 | 2 | 34 | 18 |
SI-3 | 12 | 2 | 19 | 2 | 19 | 12 |
SI-4 | 16 | 10 | 4 | 10 | 4 | 14 |
SI-5 | 16 | 10 | 40 | 10 | 35 | 14 |
SI-6 | 16 | 2 | 26 | 2 | 28 | 17 |
SI-7 | 15 | 2 | 18 | 2 | 19 | 14 |
SI-1a | 17 | 2 | 31 | 2 | 32 | 19 |
SI-2a | 14 | 10 | 24 | 10 | 20 | 14 |
SI-3a | 16 | 1 | 42 | 1 | 43 | 15 |
SI-4a | 14 | 10 | 56 | 10 | 56 | 15 |
SI-5a | 14 | 20 | 46 | 20 | 50 | 14 |
SI-6a | 12 | 5 | 10 | 5 | 12 | 13 |
SI-7a | 15 | 5 | 25 | 5 | 30 | 16 |
All synthesized SIs (SI-1–SI-7) were tested for calcite scale after thermal aging at 130 °C for 7 days.
The accuracy for all numerical values was ±5 min.
The pH of all SIs was adjusted in the range of 4–6 in 1000 ppm aqueous solution.