Table 2.
Retention time, linear range, calibration curve, limit of detection, limit of quantification, precision, stability, repeatability, and recovery of 10 reference standards.
Standard | Retention time (min) | Calibration curve | R2 | Linear range (mg L−1) | LOD (μg L−1) | LOQ (μg L−1) | Precision | Stability | Repeatability | Standard recovery rate (%) | |||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Peak area RSD (%) | Retention time RSD (%) | Peak area RSD (%) | Retention time RSD (%) | Peak area RSD (%) | Retention time RSD (%) | ||||||||
Gallic acid | 5.07 | y = 79.451x -2.9812 | 0.9999 | 0.15–15 | 0.06 | 0.41 | 1.07 | 0.47 | 0.84 | 0.06 | 0.42 | 0.06 | 98.47 |
Protocatechuic acid | 7.68 | y = 67.397x +1.481 | 0.9997 | 0.5–50 | 0.71 | 2.64 | 1.98 | 0.61 | 1.25 | 0.03 | 1.51 | 0.14 | 99.51 |
Chlorogenic acid | 9.50 | y = 39.726x -2.541 | 0.9999 | 0.8–80 | 3.22 | 10.44 | 0.94 | 0.53 | 2.71 | 0.36 | 2.25 | 0.26 | 100.71 |
Caffeic acid | 11.39 | y = 29.151x ‐ 4.516 | 0.9999 | 0.2–20 | 1.24 | 5.43 | 0.82 | 1.12 | 2.28 | 0.02 | 1.54 | 0.13 | 101.34 |
p-Coumaric acid | 15.66 | y = 129.262x +3.477 | 0.9998 | 0.6–60 | 0.03 | 1.16 | 1.17 | 0.18 | 0.87 | 0.01 | 2.26 | 0.07 | 96.72 |
Rutin | 16.68 | y = 49.814x ‐ 3.431 | 0.9999 | 0.2–20 | 1.24 | 5.37 | 1.08 | 0.36 | 1.04 | 0.01 | 3.75 | 0.06 | 98.76 |
Ferulic acid | 18.32 | y = 29.385x -1.037 | 0.9979 | 0.5–10 | 0.49 | 0.74 | 1.41 | 0.79 | 1.41 | 0.01 | 2.53 | 0.02 | 96.45 |
Salicylic acid | 30.25 | y = 89.177x +2.385 | 0.9998 | 0.7–70 | 0.15 | 0.24 | 0.97 | 0.37 | 0.79 | 0.09 | 1.65 | 0.16 | 86.92 |
Cinnamic acid | 33.87 | y = 57.221x -13.713 | 0.9998 | 0.5–50 | 0.03 | 0.22 | 1.13 | 0.06 | 1.68 | 1.26 | 1.82 | 0.14 | 96.55 |
Kaempferol | 38.42 | y = 35.216x -4.172 | 0.9999 | 0.05–5 | 0.51 | 1.57 | 3.79 | 0.09 | 1.72 | 1.96 | 2.24 | 0.38 | 105.29 |