Table 3.
Mean recoveries and standard deviations for spike concentrations of 100 and 1000 ng/mL.
| CNG Standards/ | Conc. | MRM | SIR | ||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| Mean Recovery% | (ng/mL) | Amygdalin | Amygdalin | Dhurrin | Prunasin | Linamarin | |||||
| Mean RE% | SD% | Mean RE% | SD% | Mean RE% | SD% | Mean RE% |
SD% | Mean RE% |
SD% | ||
| Sonication | 1000 | 85.40 | 1.01 | 86.14 | 1.61 | 95.34 | 2.1 | 91.35 | 0.95 | 95.26 | 1.98 |
| (30 min at 30 °C) | 100 | 91.43 | 0.92 | 92.14 | 3.11 | 88.54 | 2.04 | 79.14 | 5.1 | 92.1 | 0.96 |
| Overnight shaking | 1000 | 93.69 | 0.31 | 91.40 | 0.98 | 98.19 | 0.73 | 106.98 | 0.86 | 112.21 | 0.62 |
| (16–24 h) | 100 | 81.70 | 3.61 | 101.54 | 2.98 | 109.99 | 2.75 | 87.94 | 1.85 | 98.11 | 2.13 |