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Molecular structure of 4 in the solid state. [22] Hydrogen atoms are omitted for clarity. Selected bond lengths [Å], angles [°]: Sm1−Sb2′ 3.2375(7), Sm1−O1 2.381(6), Mo1−Sb2 2.8146(9), Mo1−Sb1 2.8549(9), Mo1−C1 1.894(8), Sb1−Sb2 2.7313(8), Sb1−Sb2′ 2.8608(7), C1−O1 1.209(10), O1‐Sm‐Sb2′ 76.73(14), Sb1‐Mo1‐Sb2 57.59(2), Mo1‐Sb2‐Sm1′ 153.18(2), Sb1‐Sb2‐Mo1 61.94(2), Sb2′‐Sb1‐Mo1 102.32(2), Sb2‐Sb1‐Sb2′ 87.73(2), Sb1‐Sb2‐Sb1′ 92.28(2).
