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Molecular structure of 5 in the solid state. [22] Hydrogen atoms and solvent molecules (toluene) are omitted for clarity. Selected bond lengths [Å] and angles [°]: Sm1−Sb1 3.2794(8), Sm1−O1 2.386(7), Mo1−Sb2 2.8464(11), Mo1−Sb1′ 2.8315(11), Mo1−C1 1.888(10), Sb1−Sb2 2.8618(10), Sb1′−Sb2 2.7254(10), C1−O1 1.221(12), O1‐Sm‐Sb1 76.8(2), Sb1′‐Mo1‐Sb2 57.37(3), Mo1‐Sb1′‐Sm1′ 152.00(3), Sb1′‐Sb2‐Mo1 61.59(3), Sb1‐Sb2‐Mo1 103.46(3), Sb2‐Sb1‐Sb2′ 90.16(3), Sb1‐Sb2‐Sb1′ 89.84(3).
