Table 2.

Particle size of hesperetin nanocrystals. I: LD data (median volume diameters (d(v)0.5 – d(v)0.95). II: PCS data (z-average and PdI)

I	particle size - LD data [µm]
	d(v)0.5			d(v)0.90			d(v)0.95			d(v)0.99
bulk	8.5	±	0.02	24.9	±	0.04	36.1	±	0.11	48.5	±	0.04
A	4.4	±	0.03	10.5	±	0.03	12.5	±	0.04	16.0	±	0.06
B	2.3	±	0.03	6.6	±	0.01	8.1	±	0.04	10.8	±	0.14
C	1.2	±	0.04	4.5	±	0.03	5.7	±	0.01	8.2	±	0.02
D	0.6	±	0.02	3.2	±	0.04	4.2	±	0.10	6.7	±	1.07
E	0.8	±	0.04	3.0	±	0.03	3.7	±	0.03	5.3	±	0.03
F	0.9	±	0.01	2.8	±	0.05	3.5	±	0.08	5.5	±	0.62
G	0.6	±	0.01	2.0	±	0.01	2.5	±	0.02	3.4	±	0.02
H	0.5	±	0.01	2.0	±	0.01	2.4	±	0.01	3.4	±	1.01
I	0.1	±	0.01	0.3	±	0.00	0.4	±	0.01	0.6	±	0.07
II	particle size - DLS data
	z-average [nm]						PdI
A	-						-
B	778			±	148		0.51			±	0.12
C	656			±	98		0.55			±	0.07
D	549			±	82		0.5			±	0.09
E	522			±	79		0.42			±	0.08
F	495			±	28		0.44			±	0.10
G	407			±	18		0.36			±	0.06
H	393			±	15		0.35			±	0.06
I	172			±	2		0.16			±	0.04