Table 1.
Interatomic Distances (Å) | ||
1 (Ln = Nd) | 5 (Ln = Dy) | |
Ln1⋯Ln1′ | 3.877 (1) | 3.795 (1) |
Ln1-O2 | 2.555 (6) | 2.453 (9) |
Ln1-O3 | 2.577 (5) | 2.499 (10) |
Ln1-O5 | 2.426 (5) | 2.343 (7) |
Ln1-O6′ | 2.404 (4) | 2.312 (8) |
Ln1-O7 | 2.503 (5) | 2.421 (8) |
Ln1-O8 | 2.578 (4) | 2.522 (8) |
Ln1-O8′ | 2.385 (5) | 2.281 (7) |
Ln1-N1 | 2.582 (6) | 2.510 (11) |
Ln1-N2 | 2.612 (5) | 2.535 (9) |
N3-O2 | 1.273 (8) | 1.289 (15) |
N3-O3 | 1.243 (8) | 1.266 (13) |
N3-O4 | 1.228 (8) | 1.230 (13) |
C8-O5 | 1.265 (8) | 1.274 (13) |
C8-O6 | 1.251 (8) | 1.253 (14) |
C10-O7 | 1.227 (8) | 1.236 (13) |
C10-O8 | 1.289 (9) | 1.293 (12) |
N1-O1 | 1.390 (7) | 1.386 (13) |
Interatomic Angles (o) | ||
N1-Ln1-N2 | 61.1 (2) | 62.9 (3) |
O2-Ln1-O3 | 49.8 (2) | 52.4 (3) |
O7-Ln1-O8 | 50.7 (2) | 52.6 (2) |
N2-Ln1-O8′ | 148.7 (2) | 147.1 (3) |
O6′-Ln1-O7 | 91.8 (2) | 90.2 (3) |
O2-Ln1-O5 | 120.4 (2) | 123.4 (3) |
O2-Ln1-O8 | 154.9 (2) | 150.1 (3) |
Ln1-O8-Ln1′ | 102.7 (2) | 104.3 (3) |
a Symmetry code: (′) = −x+2, −y+1, −z+2.