film |
soaking, 3 h in 1% trisamine solution, then 5 h in aq. solution of Zn(NO3)2∙4 H2O |
BC film removing and transfer into shallow container with 0.1 M solution of NaOH for 10 min at 50 °C |
rinse with distilled water until the composite pH became neutral, then drying |
film |
soaking, 3 h in 1% trisamine solution or DDS-Na or benzalkonium chloride for 30 min |
BC film removing and transfer into shallow container, then spraying of ZnO NPs water-alcohol dispersion onto film surface |
drying |
powder |
soaking, 3 h in 1% trisamine solution or DDS-Na or benzalkonium chloride for 30 min, sonification |
transfer into vessel, then adding of ZnO NPs water-alcohol dispersion, then sonification |
separation solid phase, rinse with distilled water until the composite pH became neutral, then drying |