Table 1.
Amine Contents, Thiol Contents, and Conversion Ratios for APTES, AHAMTES, and APDMES Treated DEa
cross-linkerb | amine contentc (μmol/mg) | thiol contentd (μmol/mg) | conv ratioe (%) |
---|---|---|---|
APTES | 1.10 ± 0.17 | 0.0312 ± 0.006 | 2.84 |
AHAMTES | 0.15 ± 0.01 | 0.0181 ± 0.003 | 12.1 |
APDMES | 0.11 ± 0.03 | 0.0130 ± 0.001 | 11.8 |
All data are reported as mean ± standard deviation for n = 3 data points unless otherwise noted. APTES thiol content was determined using n = 9 data points.
Type of aminosilane used to functionalize the surface of diatomaceous earth particles.
Primary amine content of diatomaceous earth particles after silylation.
Sulfhydryl content of silylated diatomaceous earth after NAP addition.
Ratio between sulfhydryl content after NAP addition and amine content before NAP addition.