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. Author manuscript; available in PMC: 2021 Mar 29.
Published in final edited form as: ACS Appl Mater Interfaces. 2018 Jan 11;10(3):2291–2301. doi: 10.1021/acsami.7b15967

Table 1.

Amine Contents, Thiol Contents, and Conversion Ratios for APTES, AHAMTES, and APDMES Treated DEa

cross-linkerb amine contentc (μmol/mg) thiol contentd (μmol/mg) conv ratioe (%)
APTES 1.10 ± 0.17 0.0312 ± 0.006 2.84
AHAMTES 0.15 ± 0.01 0.0181 ± 0.003 12.1
APDMES 0.11 ± 0.03 0.0130 ± 0.001 11.8
a

All data are reported as mean ± standard deviation for n = 3 data points unless otherwise noted. APTES thiol content was determined using n = 9 data points.

b

Type of aminosilane used to functionalize the surface of diatomaceous earth particles.

c

Primary amine content of diatomaceous earth particles after silylation.

d

Sulfhydryl content of silylated diatomaceous earth after NAP addition.

e

Ratio between sulfhydryl content after NAP addition and amine content before NAP addition.