Table 1.
Compounds | Quantification (µgcompound/mgsample injected ± SDs) | ||||||
---|---|---|---|---|---|---|---|
Crude extract | Hexane Fraction | DCMb fraction | EtOAcc fraction | EtOHd fraction | AcOHe fraction | Water fraction | |
Aspalathin (1) | 338.96 ± 1.90 | NDa | 0.69 ± 0.82 | 704.08 ± 12.05 | 364.98 ± 5.85 | 95.14 ± 0.91 | 191.84 ± 2.68 |
Caffeic acid (2) | 0.05 ± 0.003 | 0.02 ± 0.05 | 0.02 ± 0.05 | 0.02 ± 0.05 | 0.04 ± 0.004 | 0.04 ± 0.005 | 0.05 ± 0.004 |
Catechin (3) | 0.79 ± 0.25 | 0.36 ± 0.18 | 0.32 ± 0.17 | 1.85 ± 0.44 | 1.84 ± 0.44 | 0.32 ± 0.17 | 0.46 ± 0.19 |
Cinnamic acid (4) | 1.80 ± 0.82 | 1.00 ± 0.85 | 1.70 ± 0.82 | 2.21 ± 0.80 | 0.03 ± 0.88 | 2.15 ± 0.80 | 0.77 ± 0.85 |
Ferulic acid (5) | 0.007 ± 0.01 | 0.022 ± 0.004 | 0.424 ± 0.05 | 0.411 ± 0.05 | 0.016 ± 0.01 | 0.031 ± 0.003 | 0.034 ± 0.002 |
4-Hydroxybenzoic acid (6) | 3.07 ± 0.41 | 2.89 ± 0.38 | 0.57 ± 0.09 | 6.42 ± 0.83 | 4.02 ± 0.53 | 1.59 ± 0.22 | 4.60 ± 0.60 |
Isoquercitrin (7) | 5.07 ± 1.10 | 8.92 ± 0.89 | 134.49 ± 6.02 | NDa | 8.61 ± 0.90 | 73.50 ± 2.67 | NDa |
Luteolin (8) | 0.01 ± 0.02 | 0.02 ± 0.02 | 0.01 ± 0.02 | 0.09 ± 0.01 | 0.03 ± 0.02 | 0.06 ± 0.02 | 0.01 ± 0.02 |
p-Coumaric acid (9) | 0.001 ± 0.003 | NDa | 0.145 ± 0.06 | 0.015 ± 0.003 | NDa | 0.020 ± 0.01 | 0.001 ± 0.003 |
n-Propyl gallate (10) | 0.088 ± 0.004 | 0.088 ± 0.003 | 0.088 ± 0.003 | 0.094 ± 0.001 | 0.086 ± 0.004 | 0.085 ± 0.004 | 0.101 ± 0.001 |
Quercetin (11) | 8.61 ± 0.43 | 7.37 ± 0.47 | 0.82 ± 0.67 | 14.68 ± 0.25 | 10.46 ± 0.37 | 4.57 ± 0.55 | 10.29 ± 0.38 |
Rosmarinic acid (12) | 0.24 ± 0.09 | 0.08 ± 0.02 | 0.08 ± 0.02 | 0.11 ± 0.03 | 0.13 ± 0.04 | 0.09 ± 0.03 | 0.09 ± 0.03 |
Syringic acid (13) | 0.12 ± 0.003 | 0.09 ± 0.004 | 0.09 ± 0.004 | 0.07 ± 0.01 | 0.09 ± 0.004 | 0.09 ± 0.004 | 0.07 ± 0.01 |
Vanillic acid (14) | 0.12 ± 0.001 | 0.34 ± 0.001 | 0.24 ± 0.001 | NDa | 0.01 ± 0.001 | NDa | 0.13 ± 0.001 |
Vitexin (15) | 5.61 ± 0.59 | 6.20 ± 0.69 | 0.56 ± 0.23 | 15.95 ± 2.27 | 9.64 ± 1.25 | 4.21 ± 0.36 | 9.48 ± 1.22 |
aND not detected.
bDichloromethane.
cEthyl acetate.
dEthanol.
eAcetic acid.