Table 13.
Bond distances (Å) for compound 3.
| Bond distances (Å) | |||||
|---|---|---|---|---|---|
| C1-C6 | 1.379(5) | C13-C18 | 1.378(3) | C26-C27 | 1.372(4) |
| C1-C2 | 1.381(5) | C13-C14 | 1.381(4) | C26-N2 | 1.429(3) |
| C1-C7 | 1.518(5) | C14-C15 | 1.379(4) | C27-C28 | 1.388(5) |
| C2-C3 | 1.383(4) | C14-H14 | 0.93 | C27-H27 | 0.93 |
| C2-H2 | 0.93 | C15-C16 | 1.377(4) | C28-C29 | 1.333(5) |
| C3-C4 | 1.379(4) | C15-H15 | 0.93 | C28-H28 | 0.93 |
| C3-H3 | 0.93 | C16-C17 | 1.377(4) | C29-C30 | 1.349(6) |
| C4-C5 | 1.377(4) | C16-C19 | 1.519(4) | C29-F2 | 1.368(4) |
| C4-C8 | 1.518(4) | C17-C18 | 1.384(4) | C30-C31 | 1.385(5) |
| C5-C6 | 1.376(4) | C17-H17 | 0.93 | C30-H30 | 0.93 |
| C5-H5 | 0.93 | C18-H18 | 0.93 | C31-H31 | 0.93 |
| C6-H6 | 0.93 | C19-H19A | 0.96 | C32-O2 | 1.226(3) |
| C7-H7A | 0.96 | C19-H19B | 0.96 | C32-O1 | 1.347(3) |
| C7-H7B | 0.96 | C19-H19C | 0.96 | C33-O1 | 1.447(3) |
| C7-H7C | 0.96 | C20-N1 | 1.392(3) | C33-C34 | 1.475(5) |
| C8-N1 | 1.456(3) | C20-C25 | 1.396(4) | C33-H33A | 0.97 |
| C8-C9 | 1.536(3) | C20-C21 | 1.401(4) | C33-H33B | 0.97 |
| C8-H8 | 0.98 | C21-C22 | 1.387(4) | C34-C35 | 1.505(5) |
| C9-C10 | 1.491(3) | C21-H21 | 0.93 | C34-C36 | 1.527(5) |
| C9-H9A | 0.97 | C22-C23 | 1.362(5) | C34-H34 | 0.98 |
| C9-H9B | 0.97 | C22-H22 | 0.93 | C35-H35A | 0.96 |
| C10-N2 | 1.356(3) | C23-C24 | 1.361(5) | C35-H35B | 0.96 |
| C10-C11 | 1.365(3) | C23-F1 | 1.370(3) | C35-H35C | 0.96 |
| C11-C32 | 1.443(3) | C24-C25 | 1.382(4) | C36-H36A | 0.96 |
| C11-C12 | 1.524(3) | C24-H24 | 0.93 | C36-H36B | 0.96 |
| C12-N1 | 1.468(3) | C25-H25 | 0.93 | C36-H36C | 0.96 |
| C12-C13 | 1.528(3) | C26-C31 | 1.369(4) | N2-H2A | 0.87(3) |
| C12-H12 | 0.98 | H(2A)••••O(2) | 1.98(3) | N(2)-H(2A)••••O(2) | 2.675(3) |