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. Author manuscript; available in PMC: 2021 Mar 31.
Published in final edited form as: J Org Chem. 2021 Jan 20;86(3):2406–2422. doi: 10.1021/acs.joc.0c02546

Figure 4.

Figure 4.

Job plot showing relative integrations of the 13C{1H} resonances of NaHMDS homodimer 12 (red), NaDPTMDS-derived homodimer 22 (blue), and heterodimer 23 (green; eq 1) versus the measured29 mole fraction of NaHMDS (XNaHMDs) at 0.30 total molarity31 in neat toluene at 80 °C.