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. 2021 Mar 18;6(12):8142–8150. doi: 10.1021/acsomega.0c05936

Table 2. Effect of Solvent and Soxhlet Extractives on Lignin Extraction Systems A, B, and C.

entry system Soxhleta biomass/solvent (g/mL) isolated lignin (% yield)b
1 A N 1/10 30
2 A Y 1/10 27
3 A N 1/20 30
4 A Y 1/20 23
5c A N 1/10 27
6 Bd N 1/10 34
7 Bd N 1/20 43
8 Be N 1/10 35
9 Be N 1/20 48
10 C,170 °C N 1/10 67
11 C,170 °C N 1/20 65
a

WS pretreated with Soxhlet extraction in ethanol and water for 24 h each.

b

Based on theoretical ASL of 37 wt % of dry WS biomass.

c

Reaction under an N2 atmosphere.

d

EtOH.

e

MeOH.