Table 2. Effect of Solvent and Soxhlet Extractives on Lignin Extraction Systems A, B, and C.
entry | system | Soxhleta | biomass/solvent (g/mL) | isolated lignin (% yield)b |
---|---|---|---|---|
1 | A | N | 1/10 | 30 |
2 | A | Y | 1/10 | 27 |
3 | A | N | 1/20 | 30 |
4 | A | Y | 1/20 | 23 |
5c | A | N | 1/10 | 27 |
6 | Bd | N | 1/10 | 34 |
7 | Bd | N | 1/20 | 43 |
8 | Be | N | 1/10 | 35 |
9 | Be | N | 1/20 | 48 |
10 | C,170 °C | N | 1/10 | 67 |
11 | C,170 °C | N | 1/20 | 65 |
WS pretreated with Soxhlet extraction in ethanol and water for 24 h each.
Based on theoretical ASL of 37 wt % of dry WS biomass.
Reaction under an N2 atmosphere.
EtOH.
MeOH.