Table 1. Concentrations of Aliphatic, Carboxylic, and Phenolic OH of the hy-LNPs and the Regular LNPs According to Quantitative 31P NMR Spectroscopya.
sample | aliphatic OH | carboxylic OH | phenolic OH | total OH | wt %b |
---|---|---|---|---|---|
LNPs | 2.05 | 0.44 | 4.07 | 6.56 | 0 |
hy-LNPs10 | 2.42 | 0.35 | 3.68 | 6.45 | 10.5 |
hy-LNPs20 | 2.68 | 0.24 | 3.38 | 6.29 | 17.8 |
hy-LNPs30 | 2.34 | 0.22 | 2.73 | 5.28 | 33.6 |
hy-LNPs40* | 2.29 | 0.10 | 2.24 | 4.63 | 45.5 |
hy-LNPs50* | 2.43 | 0.04 | 1.43 | 3.91 | 65.2 |
Unit: mmol/g.
Experimental BADGE content, calculated by (1 – phenolic OH of the hy-LNPs/phenolic OH of the LNPs) × 100%.