Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1_1—H1A_1⋯Cl6 | 0.91 | 2.73 | 3.554 (19) | 151 |
| N1_1—H1A_1⋯Cl16 | 0.91 | 2.66 | 3.148 (16) | 115 |
| N1_1—H1B_1⋯Cl3i | 0.91 | 2.81 | 3.42 (2) | 126 |
| N1A_1—H1AA_1⋯Cl7 | 0.91 | 2.74 | 3.34 (4) | 125 |
| N1A_1—H1AA_1⋯Cl9 | 0.91 | 2.54 | 3.28 (3) | 138 |
| N1_2—H1A_2⋯Cl4 | 0.91 | 2.78 | 3.395 (15) | 126 |
| N1_2—H1A_2⋯O2A_5i | 0.91 | 2.48 | 3.04 (2) | 120 |
| N1_2—H1C_2⋯Cl5 | 0.91 | 2.19 | 3.101 (15) | 175 |
| N1_3—H1A_3⋯Cl10 | 0.91 | 2.69 | 3.592 (9) | 171 |
| N1_3—H1B_3⋯O2_3 | 0.91 | 2.13 | 2.605 (10) | 112 |
| N1_3—H1C_3⋯Cl2 | 0.91 | 2.53 | 3.306 (8) | 143 |
| N1_3—H1C_3⋯Cl11 | 0.91 | 2.68 | 3.228 (9) | 120 |
| N1_4—H1B_4⋯Cl15 | 0.91 | 2.44 | 3.199 (10) | 141 |
| N1_4—H1B_4⋯S1_4 | 0.91 | 2.82 | 3.300 (10) | 114 |
| N1_5—H1B_5⋯O2_12 | 0.91 | 2.36 | 3.14 (3) | 144 |
| N1_5—H1C_5⋯Cl11 | 0.91 | 2.76 | 3.46 (2) | 134 |
| N1_5—H1C_5⋯Cl13 | 0.91 | 2.49 | 3.24 (2) | 139 |
| N1A_5—H1A2_5⋯Cl2 | 0.91 | 2.74 | 3.46 (2) | 137 |
| N1A_5—H1A2_5⋯Cl11 | 0.91 | 2.42 | 2.99 (2) | 121 |
| N1A_5—H1A2_5⋯S1A_5 | 0.91 | 2.68 | 3.22 (4) | 119 |
| N1A_5—H1A3_5⋯Cl4ii | 0.91 | 2.82 | 3.49 (3) | 132 |
| N1_6—H1B_6⋯O3_6 | 0.91 | 1.92 | 2.70 (3) | 142 |
| N1_6—H1C_6⋯Cl16 | 0.91 | 2.53 | 3.311 (16) | 145 |
| N1_6—H1C_6⋯S1_6 | 0.91 | 2.89 | 3.330 (16) | 111 |
| N1A_6—H1AC_6⋯Cl11 | 0.91 | 2.74 | 3.60 (7) | 158 |
| N1_7—H1B_7⋯Cl23 | 0.91 | 2.77 | 3.435 (9) | 131 |
| N1_7—H1B_7⋯Cl26 | 0.91 | 2.58 | 3.315 (9) | 138 |
| N1_7—H1C_7⋯O1_13 | 0.91 | 1.99 | 2.803 (12) | 148 |
| N1_8—H1C_8⋯Cl26 | 0.91 | 2.51 | 3.370 (12) | 158 |
| N1_8—H1C_8⋯S1_8 | 0.91 | 2.83 | 3.286 (13) | 112 |
| N1_9—H1A_9⋯Cl20 | 0.91 | 2.85 | 3.585 (9) | 139 |
| N1_9—H1A_9⋯O1_10iii | 0.91 | 2.12 | 2.796 (11) | 130 |
| N1_9—H1B_9⋯O4_6 | 0.91 | 2.01 | 2.86 (3) | 154 |
| N1_9—H1C_9⋯Cl17 | 0.91 | 2.79 | 3.348 (9) | 121 |
| N1_9—H1C_9⋯Cl28 | 0.91 | 2.45 | 3.211 (9) | 142 |
| N1_10—H1B_10⋯Cl25 | 0.91 | 2.77 | 3.239 (9) | 113 |
| N1_10—H1B_10⋯Cl26 | 0.91 | 2.57 | 3.363 (8) | 146 |
| N1_10—H1C_10⋯O2_9iv | 0.91 | 2.15 | 2.856 (12) | 134 |
| N1_11—H1A_11⋯O1_13v | 0.91 | 2.08 | 2.971 (13) | 167 |
| N1_11—H1C_11⋯Cl21 | 0.91 | 2.61 | 3.362 (10) | 141 |
| N1_11—H1C_11⋯Cl24 | 0.91 | 2.61 | 3.235 (9) | 126 |
| N1_12—H1A_12⋯Cl31 | 0.91 | 2.92 | 3.387 (9) | 113 |
| N1_12—H1C_12⋯Cl29 | 0.91 | 2.44 | 3.316 (9) | 161 |
| O4_6—H4B_6⋯Cl12 | 0.84 (1) | 2.89 (10) | 3.32 (3) | 114 (8) |
| O4_6—H4B_6⋯O3_6 | 0.84 (1) | 1.76 (7) | 2.51 (4) | 148 (10) |
| O1_13—H1A_13⋯Cl25 | 0.82 (3) | 2.97 (3) | 3.501 (9) | 125 (2) |
Symmetry codes: (i) -x+{\script{1\over 2}}, y+{\script{1\over 2}}, -z+1; (ii) -x+{\script{1\over 2}}, y-{\script{1\over 2}}, -z+1; (iii) -x+{\script{1\over 2}}, y+{\script{1\over 2}}, -z; (iv) -x+{\script{1\over 2}}, y-{\script{1\over 2}}, -z; (v) -x+1, y, -z.