Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C6H16N2 2+·Cl4Co2− |
| M r | 316.94 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 293 |
| a, b, c (Å) | 7.6431 (3), 11.9347 (6), 14.0058 (7) |
| β (°) | 95.519 (4) |
| V (Å3) | 1271.66 (10) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.15 |
| Crystal size (mm) | 0.15 × 0.10 × 0.08 |
| Data collection | |
| Diffractometer | Agilent SuperNova, Single source at offset, Eos |
| Absorption correction | Multi-scan (CrysAlis PRO; Agilent 2014 ▸) |
| T min, T max | 0.816, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 4627, 1546, 1370 |
| R int | 0.029 |
| (sin θ/λ)max (Å−1) | 0.685 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.028, 0.074, 1.08 |
| No. of reflections | 1546 |
| No. of parameters | 60 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.27, −0.59 |