| Crystal data |
| Chemical formula |
[U(BH4)(C8H13Si)3] |
|
M
r
|
664.69 |
| Crystal system, space group |
Triclinic, P\overline{1} |
| Temperature (K) |
112 |
|
a, b, c (Å) |
8.7530 (15), 12.217 (2), 13.657 (2) |
| α, β, γ (°) |
94.159 (3), 96.016 (3), 103.256 (3) |
|
V (Å3) |
1406.6 (4) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
5.91 |
| Crystal size (mm) |
0.88 × 0.62 × 0.17 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Quest with Photon II detector |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.413, 0.747 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
30231, 10686, 9355 |
|
R
int
|
0.055 |
| (sin θ/λ)max (Å−1) |
0.769 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.037, 0.102, 1.07 |
| No. of reflections |
10686 |
| No. of parameters |
274 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
3.87, −2.72 |
