| Crystal data |
| Chemical formula |
C17H23N2O+·0.5C4H2O4
2−
|
|
M
r
|
328.40 |
| Crystal system, space group |
Triclinic, P\overline{1} |
| Temperature (K) |
297 |
|
a, b, c (Å) |
7.8791 (7), 9.2908 (7), 13.5352 (11) |
| α, β, γ (°) |
108.081 (3), 104.365 (3), 95.903 (3) |
|
V (Å3) |
894.87 (13) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.08 |
| Crystal size (mm) |
0.34 × 0.28 × 0.22 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture CMOS |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2018 ▸) |
|
T
min, T
max
|
0.711, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
27913, 3383, 2788 |
|
R
int
|
0.035 |
| (sin θ/λ)max (Å−1) |
0.611 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.043, 0.114, 1.05 |
| No. of reflections |
3383 |
| No. of parameters |
226 |
| No. of restraints |
2 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.26, −0.16 |
