| Crystal data |
| Chemical formula |
C17H19NO4
|
|
M
r
|
301.33 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
13.72487 (9), 13.05333 (9), 8.55970 (6) |
| β (°) |
95.5220 (6) |
|
V (Å3) |
1526.40 (2) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.77 |
| Crystal size (mm) |
0.08 × 0.06 × 0.05 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2020 ▸) |
|
T
min, T
max
|
0.796, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
26198, 3125, 2975 |
|
R
int
|
0.025 |
| (sin θ/λ)max (Å−1) |
0.625 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.033, 0.090, 1.03 |
| No. of reflections |
3125 |
| No. of parameters |
202 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.27, −0.18 |
