Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C25H22N2O3S·0.04H2O |
| M r | 1724.87 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 12.049 (2), 20.223 (4), 9.1743 (18) |
| β (°) | 100.91 (3) |
| V (Å3) | 2195.0 (8) |
| Z | 1 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.18 |
| Crystal size (mm) | 0.36 × 0.03 × 0.03 |
| Data collection | |
| Diffractometer | Bruker D8 QUEST PHOTON-III CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.930, 0.990 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 40890, 4492, 3208 |
| R int | 0.086 |
| (sin θ/λ)max (Å−1) | 0.625 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.043, 0.099, 1.02 |
| No. of reflections | 4492 |
| No. of parameters | 297 |
| No. of restraints | 7 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.24, −0.28 |