Table 3. Cycloisomerization of S3 Using Recycled C1 and C2a.
Reaction conditions: 0.4 mmol of S3, 0.08 mmol of triethylamine, 0.012 mmol of Pd(II)-AmP-MCF, and 1 mL of toluene. The NMR yield was determined using 1,3,5-trimethoxybenzene as the internal standard.
1 mol % BQ used to reactivate the catalyst before the reaction.
1 mol % BQ added at the beginning of the reaction.
