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Experimental parameters for data acquisition for the NMR experiments.
| Parameter | COSY | 13C-HSQC | HMBC | NOESY | 1H | 13C-HSQC-AP |
|---|---|---|---|---|---|---|
| Relaxation delay [s] | 1 | 1.5 | 1 | 6 | 1 | 1.5 |
| Number of transients | 4 | 2 | 4 | 4 | 8 | 8 |
| Acquisition time [s] | 0.15 | 0.15 | 0.15 | 0.15 | 1.7 | 1.2 |
| Number of increments | 200 | 300 | 200 | 200 | n.a. | 400 |
